Effect of Mechanical Activation on Ti3AlC2 Max Phase Formation under Self-Propagating High-Temperature Synthesis

  • A. Yu. Potanin National University of Science and Technology “MISIS”, SHS Research & Education Center MISIS-ISMAN, Leninsky prospect, 4, Moscow, 119049, Russia
  • P. A. Loginov National University of Science and Technology “MISIS”, SHS Research & Education Center MISIS-ISMAN, Leninsky prospect, 4, Moscow, 119049, Russia
  • E. A. Levashov National University of Science and Technology “MISIS”, SHS Research & Education Center MISIS-ISMAN, Leninsky prospect, 4, Moscow, 119049, Russia
  • Yu. S. Pogozhev National University of Science and Technology “MISIS”, SHS Research & Education Center MISIS-ISMAN, Leninsky prospect, 4, Moscow, 119049, Russia
  • E. I. Patsera National University of Science and Technology “MISIS”, SHS Research & Education Center MISIS-ISMAN, Leninsky prospect, 4, Moscow, 119049, Russia
  • N. A. Kochetov Institute of Structural Macrokinetics and Materials Science, Russian Academy of Sciences, str. Academica Osipyana, 8, Chernogolovka, Moscow Region, 142432 Russia
Keywords: SHS, mechanical activation, mechanosynthesis, Ti3AlC2, combustion rate

Abstract

In this study, we have investigated the effect of various mechanical activation (MA) modes on phase and structure formation in powder mixtures made up to produce Ti3AlC2 MAX phase. The optimal MA duration has been established which results in the maximum heat release under SHS due to accumulation of structural defects leading to the growth of internal energy. The effect of MA on the character and kinetics of combustion front propagation has been investigated. It was shown that following pretreatment of a powder mixture in a planetary ball mill, the combustion mode changes from stationary to a pulsating combustion and, consequently, the combustion rate decreases. The burning-out of the sample is partial and with
interruptions (depressions). Force SHS-pressing technology was used for obtaining of compacted samples with homogeneous structure based on Ti3AlC2.

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Published
2015-07-20
How to Cite
[1]
A. Potanin, P. Loginov, E. Levashov, Y. Pogozhev, E. Patsera, and N. Kochetov, “Effect of Mechanical Activation on Ti3AlC2 Max Phase Formation under Self-Propagating High-Temperature Synthesis”, Eurasian Chem. Tech. J., vol. 17, no. 3, pp. 233-242, Jul. 2015.
Section
Articles