Atomic-Emission Determination of Rhenium in Anthropogenic Raw Materials of Steel Production

Authors

  • A. V. Troeglazova Department of Chemistry, al-Farabi Kazakh National University, Almaty, Kazakhstan
  • E. V. Zlobina Department of Chemistry, al-Farabi Kazakh National University, Almaty, Kazakhstan
  • G. S. Kudryavtseva «Giredmet» State Scientific-Research and Design Institute of Rare MetalIndustry, Moscow, Russia
  • A. D. Kirillov «Giredmet» State Scientific-Research and Design Institute of Rare MetalIndustry, Moscow, Russia
  • Y. A. Karpov «Giredmet» State Scientific-Research and Design Institute of Rare MetalIndustry, Moscow, Russia

DOI:

https://doi.org/10.18321/ectj213

Abstract

The method including microwave acidic dissolution of samples and atomic-emission analysis of rhenium for determination of rhenium in cupper-molybdenum and lead-cupper wares is proposed. The range of determination concentration of metal is 0.05 – 0.5 mass percent, standard deviation of repeatability is 0.002 – 0.01%.

References

1. Palant A.A., Troshkina I.D., Chekmarev A.M. Metallurgy of rhenium. Moscow: Nauka, 2007, 298 р.

2. Borisova L.V., Ermakov A.N. Analytical chemistry of rhenium. Moscow: Nauka, 1974, 321 р.

3. Naumov A.V. Rhythms of rhenium (review of world market) // Proceedings of the universities. Non-ferrous metallurgy. 2007. – № 6. – P. 36-41.

4. Karpov Y.A., Savostin A.P. Methods of sampling and sample preparation. Moscow: BINOM. Knowledge Lab, 2003. – 243 p.

5. Vasilyeva L.N., Karpov Y.A., Shiryaeva O.A. Modern methods for determination of rhenium // Non-ferrous metals, 1991. - №7. - P. 44-49.

6. Borisova L.V., Fabelinskiyi Y.I., Plastinina E.I., Prasolova O.D. Extraction-atomic emission with inductively coupled plasma method for determination of trace amounts of rhenium in copper sulfide samples // Factory laboratory, 1990. - №12. – P. 10-12.

7. Ryazanova L.N., Shiryaeva O.A., Nikitenko M.O. Determination of rhenium in copper ores and products of their concentration by atomicemission method with induction plasma // Factory laboratory,1990. - №12. – P. 8-10.

8. Kubrakova I.V. Microwave radiation in analytical chemistry: opportunities and prospects of using // Advances in the Chemistry. 2002. - № 4 (71). – P. 327-339.

9. Karpov Y.A., Orlova V.A. Modern methods of autoclave sample preparation in chemical analysis of substances and materials // Factory laboratory. Diagnosis of materials, 2007. – V.73 – № 1 – P. 4-11.

10. V. Camel. Trends in Anal. Chem., V. 19, № 4, P. 229 (2000).

11. ISO 5725:1994. Accuracy (trueness and precision) of measurement results, Part 1-6: Basic method for repeatability and reproducibility of a standard measurement method, ISO, Case postale 56, CH-1211, Genève 20, Switzerland.

12. EURACHEM/CITAC Guide Quantifying Uncertainty in Analytical Measurements. Second Edition. 2000.

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Published

2011-12-22

How to Cite

Troeglazova, A. V., Zlobina, E. V., Kudryavtseva, G. S., Kirillov, A. D., & Karpov, Y. A. (2011). Atomic-Emission Determination of Rhenium in Anthropogenic Raw Materials of Steel Production. Eurasian Chemico-Technological Journal, 13(3-4), 241–245. https://doi.org/10.18321/ectj213

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